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Hydrogen bonded supramolecular framework in a monoclinic polymorph of (E)-2-(1-(2-phenylhydrazono)ethyl)phenol
Author(s): A. L. AmruthaKala, Karthik Kumara, M. Prabhuswamy, G. Pavithra, K. Ajay Kumar and N. K. Lokanath
Schiff base of 2-acetylphenolwas synthesized by the reaction of 2-acetylphenol and phenylhydrazine hydrochloride in the presence of sodium acetate in ethyl alcohol under reflux conditions. The crystal structure of the title compound was determined and analyzed by single crystal X-ray diffraction studies. The compound crystallizes in the monoclinic crystal system with space group P21 /n and unit cell parameters, a = 13.409 (4) Å, b = 10.665 (3) Å, c = 17.688 (4) Å; β=109.2(8)° and Z = 8. The crystal and molecular structure of the title compound is stabilized by the O—H···N and N—H···O hydrogen bond interactions.