Comparative study of X-ray diffraction patterns of transition metal complexes like Cu (II), Co (II) and Zn (II) of thiosemicarbazone is carried out. These metal complexes have different physicochemical properties as well as different crystal system. The X-ray diffraction studies were also being used for the determination of various parameters such as unit cell volume and miller indices values h, k, l. These complexes also tested for their antibacterial and antifungal activity in comparison with standard drug ciprofloxacin.
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